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Beilstein J. Org. Chem. 2015, 11, 980–993, doi:10.3762/bjoc.11.110
Graphical Abstract
Figure 1: PV-PTFE reaction design.
Figure 2: Solvent uptake in the delivery of bromine into dichloromethane (a) 0 min, (b) 0.50 min, (c) 0.83 mi...
Figure 3: Solvent column heights of bromine delivery into dichloromethane (○) and ethyl acetate. (♦).
Figure 4: Reproducibility of bromine delivery into a) dichloromethane and b) ethyl acetate. In each case thre...
Figure 5: Height of the solvent column in the course of the bromination of cyclohexene in (a) dichloromethane...
Figure 6: Height of the solvent column in the course of the bromination of cyclohexene in ethyl acetate (♦) a...
Figure 7: Solvent uptake when the delivery tube is inserted to a shallow depth. The solvent uptake stopped on...
Scheme 1: Iodolactonization of unsaturated diester 1 with iodine monochloride in dichlormethane.
Figure 8: (a) The delivery tube is immersed into the solution and there is a considerable solvent uptake. (b)...
Figure 9: Transport of dyed dimethyl phthalate in dichloromethane after (a) 0 h, (b) 1 h, (c) 2 h, (d) 3 h an...
Figure 10: Transport of dyed dimethyl phthalate in ethyl acetate after (a) 0 h, (b) 0.17 h, (c) 1 h, (d) 3 h, ...
Scheme 2: Chemiluminescence reaction of diaryl oxalate esters oxidized by hydrogen peroxide in the presence o...
Figure 11: When the diaryl oxalate was oxidized by aqueous peroxide solution, chemiluminescence was observed o...
Figure 12: Progression of PV-PTFE chemiluminescence with aqueous peroxide solution in the vial after (a) 10 mi...
Figure 13: Progression of PV-PTFE chemiluminescence with acetonitrile–aqueous peroxide solution in the vial af...
Figure 14: Diffusion of dimethyl phthalate assisted by tert-butanol through PTFE was visualized in a chemilumi...
Figure 15: Corrosion of aluminum resulting from bromine applied directly to metal.
Figure 16: Discoloration of aluminum from bromine applied to PTFE tape on metal.
Figure 17: After stirring bars were cut open, some iron bars were found to be corroded.
Figure 18: (a) Diffusion of bromine through a bulk PTFE from stirring bar into dichloromethane after 2 h. (b) ...
Figure 19: Diffusion of bromine through a PTFE tube.
Figure 20: (a) The reaction of benzene and bromine in the absence of a stirring bar (), in the presence of a n...